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Frigmaires Engineers
Mumbai, Maharashtra, India
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Our Products

  1. Filling Line 4 Products available
  2. Grinding Mill 7 Products available
  3. Milling Machines 7 Products available
  4. Chemical Machinery & Plant 9 Products available
  5. Dryers 3 Products available
  6. Grinding & Milling Tools & Machinery 13 Products available
  7. Construction Machinery & Equipment 13 Products available
  8. Powder Mixers 5 Products available
  9. Others 60 Products available

Chemical Machinery & Plant #817977

Bitumen Plant

We offer complete Bitumen Emulsion Manufacturing Plant MS.RS and SS grade of emulsions as per Is 8887 on turnkey basis along with erection & commissioning. Our dedicated team of engineers works closely with our customers to ensure that the entire process of setting up the Bitumen Plant is made uncomplicated. Apart from training your chemists we also provide technical and commercial support for a period of 12 months from date of commissioning the plant. Capacity Offered5MT/batch TO 25MT/batch size plantUsesBuilding of roads, runways and platformsWater proofing Mastic floorings for factories and godownsCanal coating which stops erosionDump-proofingTank baseJoint filling materialFeaturesLong lastingEasy to install and operateCustomized as per requirements
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Lab Grease Plant

The Lab Grease Plant We Manufacture and Export is Used to Make Calcium/lithium/soda Base Grease from 10kgs to 100kgs / Batch. Lab Grease Plant is Economically Priced and Offers High Performance. the Lab Grease Plant is Robust and Highly in Demand in the Market.
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Disperser

We are offering disperser.the disperser manufactured at frigmaires engineers is a highly versatile machine for the production of paints, inks, coatings, construction chemicals etc. The main function of the disperser is breaking up of the agglomerates, wetting & dispersing of pigments in liquids. A wide range of paints & inks can be produced on our dissolvers without the use of grinding media. We offer the disperser in various dimensions and keeping in view clients requirement. advantages :saves power because of the variable speed control as the speed of the shaft can be diverse at various stages of the mixing process.offers uniform product circulation as well as perfect dispersion due to proper hydraulic lifting and lowering alignment. Herein, the height of the mixing shaft can be easily adjusted. Optional available :flame proof fittingsvacuum arrangementmixing vesselselectronic ac frequency drive that vary rpm from 0 3000technical specifications

MODELWORKING CAP. IN LTRS.MOTOR HPRPMCAPACITY OF VESSELS IN LTRS.
FD-12507.50 - 1500 350
FD-2500100 - 1500 700
FD-3100020/300 - 1500 1400
FD-4200040/500 - 1500 2800
FD-5300050/750 - 1500 4200
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Resin Plant

For installation of Resin Plant, we employ extremely knowledgeable technologists who have hands on experience in the related field. Our dedicated team of engineers works closely with our customers to ensure that the entire process of setting up the Resin Plant is made simple. Apart from training your chemists, we also provide technical and commercial support for a period of 12 months from date of commissioning the plant. Used to manufacture Alkyd resinPVA emulsionCapacity OfferedFrom Lab Size to 10MT batch plantFeaturesHigh performanceDurableHigh tensile strengthEconomical
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Grease Plant

  • Basic Types Of Grease  
  • SOAP TYPES GREASES NON SOAP THICKNER GREASES
  • Metallic soaps + Lubricating Oils + Additives for imparting Special properties Thickening Agent + Lubricating Fluid (Synthetic oils) + Additives for imparting Special properties

Types Of Greases

Lithium, Calcium, Soda, Aluminium, Complex and Mixed soap base Greases, Soap free Grease, PTFE, Silicone and Molybdenum modified Greases, Specialty and Synthetic Greases.

Basic Defination

The original Definition of ASTM of Grease was "A solid or semi solid combination of petroleum products and a soap or mixtures of soaps with or without fillers, suitable for certain types of lubrication.

Subsequent technological advances have led to the use of synthetic lubricating fluids on the one hand and non-soap thickeners on the other hand.

Current - Modified Definition of Grease is "A solid or semi solid product of dispersion of thickening agent in liquid lubricant. Other ingredients imparting special properties may be included.

Most greases are in fact is a combination of petroleum oils and metallic soaps.

Grease is a lubricant of higher initial viscosity than oil, consisting originally of a calcium, sodium or lithium soap jelly emulsified with mineral oil.

Greases are typically used in areas where a continuous supply of oil cannot be retained, such as open bearings or gears.

Grease is a fine dispersion of an oil-insoluble thickening agent - usually soap in a fluid lubricant which is generally mineral lubricating oil. The soap is made up of fatty acid, tallow or vegetable oil saponified with alkali which can be hydrated lime, caustic soda, lithium hydroxide or aluminum hydroxide. The lubricating oil component is refined base oil-naphthenic, of medium viscosity index, or cylinder oil stock. Structurally grease is a water-in-oil emulsion. Its appearance is smooth, mostly translucent, soft or hard.

Properties essential for performance of grease are structural stability, lubricating quality, low and high temperature performance (which are provided by the selected lube oil base stock), where as properties such as water resistance, high temperature quality, resistance to break down through continuous use and ability of grease to stay in place are provided by the soap.

Additives e.g. Graphite, modified clay, asphalt, oxidation and corrosion inhibitors, extreme pressure additives molybdenum disulphide etc. are used to impart specific properties as required by end application.

Factors to be considered when selecting greases are the type of grease, which in turn depends on operating temperatures, water resistance, oxidation stability etc. The second factor, no less important, are the grease's characteristics, including viscosity and consistency.

The value of plastic lubricants has been recognized since very early times when animal fats were used for Axles and the like.

In general any lubricating fluid can be gelled by means of a suitable thickness to form a lubricating Grease. In practice mineral oils are almost exclusively used. For soap type Greases mineral oils of relatively low viscosity index 60 are preferred since the greater solvency of the more aromatic oils for soaps makes manufacture easier and gives greases with lower soap contents and with better properties.

Synthetic Fluids: Esters and silicones are used, only in greases for special applications, where cost is secondary to performance to meet low temperature and high temperature requirements; - 75C to + 320C.

The Soaps used are the metallic salts of long chain fatty acids derived from wide range of natural fatty materials. Soaps are mainly produced by specifying the fat or fatty acid with appropriate alkali in the presence of oil.

In some cases pre-formed soaps are used, such as aluminium stearate, lithium sterate etc.

Non Soap Thickners may be inorganic e.g. silica or clay or organic with a very high melting point . e.g. terephthalamates, arylureas (these may be either pre-formed or formed in situ) and the dye stuffs, indanthrene and phthalscyanine. They need to be oleophilic and this characteristic may be imparted either in the thickner formulation (i.e. by including a long chain hydrocarbon chain or surface esterification ) or by coating the particle surfaces with organic cations. In the latter case about 75 percent of the particle surface is covered, which gives the desired effect without affecting inter particle forces too much. Pre-treated clays (i.e. coated and dried) need aids to facilitate dispersion in oil. These dispersion aids are low molecular weight polar organic compounds such as methanol, acetone, diacetone Alcohol and propylene Carbonate.

A satisfactory Grease for a given application is expected to:

  1. Provide adequate lubrication to reduce friction and to prevent harmful wear of bearing components
  2. Protect against corrosion
  3. Act as a seal to prevent entry of dirt and water.
  4. Resist leakage dripping or undesirable throw off from the lubricated surfaces.
  5. Resit objectionable change in structure or consistency with mechanical working (in the bearing) during prolonged services.
  6. Not stiffen excessively to cause undue resistance to motion in cold weather.
  7. Have suitable physical characteristics for the method of application.
  8. Be compatible with elastomer seals and other materials of construction in the lubricated portion of the mechanism.
  9. Tolerate some deqree of contamination, such as moisture, without loss of significant characteristics.

Soap Greases consist of dispersions of soap fibres in oil in concentrations mostly in the range 5 to 22%. By weight sometimes solid block greases contain 50 to 40% of soap.

The thickeners in non-soap greases are usually particulate rather than fibrous in nature and in this case the structure is maintained by 3 dimensional linkages due to very short range inter particle forces (Vander waals forces). These linkages are readily broken and re-formed.

Types Of Greases

The metallic radical of the soap largely determines the characteristics of the greases the fatty radical having a secondary effect. Greases are therefore classified in terms of the metal they contain.

Calcium Soap Greases Sodium Soap Greases

The conventional types ( excluding the complex soap greases have a smooth buttery texture and are water resistant, with dropping points around 90- 100 C. They are water stabilized, that is , the water is present in the soap crystals as water of crystallization. The optimum amount of water varies considerably with the type of formulation, fatty material and mineral oil used, but is usually within the range of 0.5 1.3% by wt. at high temperatures the water is gradually lost and the soap structure is weakened. Consequently, calcium soap Greases are restricted to use at fairly low maximum temperatures about 50 60C. They all turn fluid after exposure to high temperatures and may separate into the oil and soap phases. Only those which contain other stabilizers besides water ( e.g. wool grease) will regain their structure on cooling.

These are usually more or less fibrous in structure/ texture depending mainly on the nature of the fatty material, high unsaturation yielding very fibrous greases. They have high dropping points usually not less than 150C and sometimes as high as 200C and are useful for relatively high temperature service. Owing to the solubility of the soap in water they are not water resistant.

 
Lithium Soap Greases Aluminium Soap Greases

These greases first appeared during -the World War II and were made from Lithium Stearate preformed soap. Now a-days lithium hydroxy stearate greases made by saponification in situ from hydrogenated castor oil predominate. Depending on the composition Lithium greases are smooth or slightly grainy in appearance. They have the highest dropping point about 190C of the conventional greases and the highest service temperatures. They are water resistant, mechanically stable, and can be made with a greater variety of types of oil than other greases. Their versatility and wide operational scope especially in high-speed service has led to their use as Multipurpose greases to the displacement of earlier types of more specialized greases.

Aluminium Greases have an attractive translucent smooth and polished appearance. The dropping points are low about 90C and the greases tend to become rubbery at high temperatures. They are almost invariably made from high viscosity oils and often incorporate polymers. Such products are water Resistant; stringy, and adhesive, and find application as chassis and gear lubricants. They are not recommended for rolling bearings.

 
Mixed Soap Greases Complex Soap Graeses

A variety of mixture is used, the commonest being Sodium-Calcium and the greases are generally manufactured by saponifying the fatty materials with mixed alkalies derived from different metals. One of the soaps usually predominates and determines the general character of the grease, while the other modifies the structure in some way. This results for example, in changes in texture and improved mechanical stability.

The normal soaps can be complexed with various inorganic salts, usually short-chain aliphatic compounds. The commonest type is a calcium soap calcium acetate complex although many other combinations have been patented. The greases are water resistant and have very high dropping points, in the range 200 -300C. With EP additives incorporated they are encountered as steel mill greases. New greases have recently been introduced for multi-purpose.

 
Non- Soap Greases

There are two main types, these intended for general industrial use and those for specialized applications. The former include greases thickened with silica and clay ( Bentonite) and organic derivatives,such as terephthalamates, diamido dicarbonyl and aryl substituted ureas. High temperatures, mechanical stability, water resistant etc. suggest that they are multipurpose greases with a wider scope than soap greases. However, they have not made any great impact on the market. The type used for specialized applications includes greases made from the dye stuffs indanthrene and phthalocyanine which are generally combined with synthetic fluids, such as diesters and silicones and hence are very expensive. One such product is claimed to operate between - 75C and + 320C.

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Solvent Based Resin Plants

What is Resin ?

Resins are film forming materials used in the production of paints and coatings. It binds the pigment particles into a coherent film that adheres to the substrate. The quality of the resin used in the production of paints and coating decides the durability of the paint. Resins are used depending upon the functional properties of the paint.

Functions of Resin:

To provide gloss and elasticity.

For the suspension of pigments.

To provide resistance to water, chemicals and abrasion.

Makes coating adhere to the surface.
Acts as a dispersant.
For drying properties.

Alkyd resins from the largest group of synthetic resins are used in paint industry. Most air drying enamels are based on long or medium oil alkyd resins. These resins dry at room temperature and have excellent flow and leveling properties, good exterior durability and can be thinned with mineral turpentine. Oils used for producing alkyd resins are linseed oil, soybean oil and Dehydrated Castor Oil (DCO).

Plant Operations:

Frigmaires solvent based plant produces paints, coatings, stains, and surface treating products at a rate of about 1.1 million gal/yr. This paint manufacturing plants operations primarily involve blending and mixing of raw materials, product testing and packaging and cleaning of vessels and lines. Color separation of the product is done to befit customer specifications.

Water-based and solvent-based paints are mixed in different tanks from 200- to 1000-gal capacity. The material used in water-based paints include water, latex, resins, extenders, and dispersed pigments. For solvent-based paints, the materials are generally similar in type, but solvent replaces water and latex. Other ingredients used in this base include plasticizers, tints, and thinners.

After batches are made up, they are transferred to the let-down tanks. Additional water (or solvent), resins, preservatives, anti-foaming agents, thinners, and bactericides are added thereafter in the tanks. Batch testing encompasses checking color, viscosity and gloss. The material are then filtered and charged to cans for labeling, packaging, and shipping.

Waste Generation:

The principal waste streams are the result of equipment cleaning, especially from water-based paints. For example, rinsing the let-down tanks ordinarily requires about 35 gal of rinse water, but that amount increases to 53 gal if light paint is to be blended after dark paint. The hazardous nature of water rinses results from the mercury used as a bactericide in the paint.

The rinses are separated from the paints according to the color intensity. Waste rinses that are not reused are piped to holding and flocculation tanks, after that alum is added to lower the pH and flocculent is added to precipitate some solids. Finally, the supernatant liquid is removed for reuse in other paint formulations.

The tanks are rinsed with mineral spirits at a rate of about 5 gal/400-gal tank. There after, the washings are sent off-site for recovery, followed by recycling or sale as fuel.

Waste Minimization;

In addition to reusing rinse water and recovering solvent, following measures to reduce waste generation are specified below :

Cleaning of the equipment before paint dries and hardens.
Eliminating hazardous materials.
Avoiding hazardous container waste by collecting the bactericide in water-soluble bags.
Scheduling batch formulations so that light colored paints precede dark ones.

Reducing the inventory of raw materials to avoid degradation and spoilage and to ensure a high-quality product.

Using bag filters for collecting dust.

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Acralic Resin Plants

What are Emulsions:

Emulsions are solvent free binders used in the preparation of paints and coatings. These are produced by the polymerization process where monomers are dispersed in an aqueous phase to get a uniform and stable emulsion. Paints and coatings based on emulsion systems are best in performance and are environment friendly.

Functions of Emulsion:

Excellent binding and hardness properties.
Makes the paint elastic.
Better sheen and gloss.
Excellent U.V. resistance.

High pigment loading capacity.

Acrylic Emulsion in Paints:

Different types of emulsions used in paints are pure and styrene acrylic emulsions. These emulsions are economical and are easily available. Emulsion based paints are free of solvents and are fast replacing solvent based paints due to its functionality and environmental friendly properties.

Manufacturing Process:

The processes involved in the formation of acrylic emulsion resin are complex and vary extensively. The production of low molecular weight dispersant product generates significant quantities of wastes.

Acrylic Emulsion Production:

Different acrylic emulsion formulations are produced by frigmaires acrylic emulsion resin plant. The steps involved in acrylic emulsion production varies greatly from product to product. Steps involved in the production of acrylic emulsion are listed below:

Raw materials for the emulsion line include monomers, additives, activators, and catalysts in liquid or solid form. For stabilization, some monomers are pre-mixed with inhibitors.

Catalysts are used for activating the monomers and initiating the desired reactions. Activators activate the catalysts, initiates the reaction, besides overcoming the effects of the inhibitors. Additives used in the mixture include detergents, dispersants, and pH-adjustment ingredients.

There after, the monomers are pumped from tanker trucks to monomer tanks for storage.

From the storage tanks, monomers are pumped to holding / premixing tanks, additive, activator, and catalyst holding tanks where mixing occurs.

The additives, activators, and catalysts can be directly added to the reactors without being mixed with monomers in their respective holding tanks.

Then, the raw materials are mixed together in one of three temperature- and pressure-regulated reactors where polymers are formed. The desired chemical reactions are initiated by addition of catalysts and are regulated with additives or by pressure and temperature adjustment.

The resulting acrylic emulsion polymers are pumped to blend tanks. Formalin is added in the blend as a preservative to control bacteria and mold growth and ammonia is added to for pH adjustment. Sodium hydroxide is another pH-adjustment chemical, added in the blend tanks.

Ingredients such as emulsions, emulsifiers, surfactants, binders and thickeners are added to modify monomer viscosity, to stabilize the polymers and to hold the polymers in suspension.

Finally, deionized water is added to lower the solids content. After each polymer batch is processed, the blend tanks are flushed with deionized water which is further pumped to the plant's wastewater treatment system.

Wastes generated during different processes include composited absorbed monomers, burnable liquids, and off grade methylolacrylamide / acrylamide. Most of the composited absorbed monomer waste are generated from spillage during loading and unloading of the rail cars or from batch spills and reactor clean-ups.

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Multipurpose Resin Plants

Pilot Plant:

Multipurpose Resin Plants are the pilot plants of Frigmairies. The structural design, configuration and material of construction of our plants can be custom made to suit the distinct requirements of our clients. These plants can produce both solvent and acrylic based resins.

Capacities of our Multipurpose Resin Plant range from 10 to 100 Ltrs. / Batch. Frigmairies can provide operation and installation support at the client's location, if required. Our design and technical engineers assist you about the proper functionality of our plant.

The precision configuration of our Multipurpose Resin Plant are specified below:
Reactors:

The reactors that are configured in our plant are manufactured as per ASME codes. These reactors are developed from superior quality stainless steel ranging from 1000 Ltrs. The capacity of these reactors is Upto 2, 000 ltrs. Specially designed agitators with heating coils / jackets upto 350C are configured in our reactors. Internal colding can also be taken care.

Heat Exchangers:

Thermic fluid heating systems upto 3 Million KCAL / Hr with all ancillary equipment and safety requirements are offered by us. Further, we also provide steam generators, having capacity of 1000 Kgs / Hr.

Condenser:

We provide you with distinct choices in the condenser types, to befit our customer's requirements. These can be configured in the plant to befit your specific requirement. The material of construction of these condensers can also vary in accordance to distinct need.

We offer following choices in our condensers :
View Larger image
Shell & Tube, U Bundle Type
Fixed or Floating Head Type
Double Pipe Coolers
M.O.C: Stainless Steel, Carbon Steel, Monel, Nickel Aluminum
Filtering:

Specially designed filtering units for micron size filtering are incorporated on our plants. The resins and emulsions that are produced in Frigmairies Multipurpose Resin Plant comply with the industrial standards. The waste material generated during the production process is efficiently filtered and separated with the help of these filtration units.

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Sigma Kneader

Excellent for kneading and mixing of highly viscous materials like dough, putty, rubber solutions, adhesives, polymers etc. The mixing action is a combination of smearing, stretching, folding, dividing and recombining as the material is processed between the sigma blades and the container walls. Jacket arrangement is provided for heating or cooling application. In bigger models the container is tilted by a hydraulic cylinder to ensure complete discharge of mass.

MODEL TOTAL VOLUMETRIC CAP. IN LTRS. HP HYDRAULIC TILTING HP
SK 6 6 1.5 N.A
SK 25 25 3 N.A
SK 50 60 5 N.A
SK 125 125 10 N.A
SK 225 225 20 1.5
SK 500 500 30 2
SK 1000 1000 60 3
SK 1500 1500 75 3
SK 3000 3000 300 7.5
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Retailer of Chemical Machinery & Plant from Mumbai, Maharashtra by Frigmaires Engineers
Post Buy Requirement
Frigmaires Engineers
Mumbai, Maharashtra, India
Add Review

Our Products

  1. Construction Machinery & Equipment 13 Products available
  2. Powder Mixers 5 Products available
  3. Filling Line 4 Products available
  4. Grinding Mill 7 Products available
  5. Milling Machines 7 Products available
  6. Chemical Machinery & Plant 9 Products available
  7. Dryers 3 Products available
  8. Grinding & Milling Tools & Machinery 13 Products available
  9. Others 60 Products available

Chemical Machinery & Plant #817977

Bitumen Plant

We offer complete Bitumen Emulsion Manufacturing Plant MS.RS and SS grade of emulsions as per Is 8887 on turnkey basis along with erection & commissioning. Our dedicated team of engineers works closely with our customers to ensure that the entire process of setting up the Bitumen Plant is made uncomplicated. Apart from training your chemists we also provide technical and commercial support for a period of 12 months from date of commissioning the plant. Capacity Offered5MT/batch TO 25MT/batch size plantUsesBuilding of roads, runways and platformsWater proofing Mastic floorings for factories and godownsCanal coating which stops erosionDump-proofingTank baseJoint filling materialFeaturesLong lastingEasy to install and operateCustomized as per requirements
View Complete Details

Lab Grease Plant

The Lab Grease Plant We Manufacture and Export is Used to Make Calcium/lithium/soda Base Grease from 10kgs to 100kgs / Batch. Lab Grease Plant is Economically Priced and Offers High Performance. the Lab Grease Plant is Robust and Highly in Demand in the Market.
View Complete Details

Disperser

We are offering disperser.the disperser manufactured at frigmaires engineers is a highly versatile machine for the production of paints, inks, coatings, construction chemicals etc. The main function of the disperser is breaking up of the agglomerates, wetting & dispersing of pigments in liquids. A wide range of paints & inks can be produced on our dissolvers without the use of grinding media. We offer the disperser in various dimensions and keeping in view clients requirement. advantages :saves power because of the variable speed control as the speed of the shaft can be diverse at various stages of the mixing process.offers uniform product circulation as well as perfect dispersion due to proper hydraulic lifting and lowering alignment. Herein, the height of the mixing shaft can be easily adjusted. Optional available :flame proof fittingsvacuum arrangementmixing vesselselectronic ac frequency drive that vary rpm from 0 3000technical specifications

MODELWORKING CAP. IN LTRS.MOTOR HPRPMCAPACITY OF VESSELS IN LTRS.
FD-12507.50 - 1500 350
FD-2500100 - 1500 700
FD-3100020/300 - 1500 1400
FD-4200040/500 - 1500 2800
FD-5300050/750 - 1500 4200
View Complete Details

Resin Plant

For installation of Resin Plant, we employ extremely knowledgeable technologists who have hands on experience in the related field. Our dedicated team of engineers works closely with our customers to ensure that the entire process of setting up the Resin Plant is made simple. Apart from training your chemists, we also provide technical and commercial support for a period of 12 months from date of commissioning the plant. Used to manufacture Alkyd resinPVA emulsionCapacity OfferedFrom Lab Size to 10MT batch plantFeaturesHigh performanceDurableHigh tensile strengthEconomical
View Complete Details

Grease Plant

  • Basic Types Of Grease  
  • SOAP TYPES GREASES NON SOAP THICKNER GREASES
  • Metallic soaps + Lubricating Oils + Additives for imparting Special properties Thickening Agent + Lubricating Fluid (Synthetic oils) + Additives for imparting Special properties

Types Of Greases

Lithium, Calcium, Soda, Aluminium, Complex and Mixed soap base Greases, Soap free Grease, PTFE, Silicone and Molybdenum modified Greases, Specialty and Synthetic Greases.

Basic Defination

The original Definition of ASTM of Grease was "A solid or semi solid combination of petroleum products and a soap or mixtures of soaps with or without fillers, suitable for certain types of lubrication.

Subsequent technological advances have led to the use of synthetic lubricating fluids on the one hand and non-soap thickeners on the other hand.

Current - Modified Definition of Grease is "A solid or semi solid product of dispersion of thickening agent in liquid lubricant. Other ingredients imparting special properties may be included.

Most greases are in fact is a combination of petroleum oils and metallic soaps.

Grease is a lubricant of higher initial viscosity than oil, consisting originally of a calcium, sodium or lithium soap jelly emulsified with mineral oil.

Greases are typically used in areas where a continuous supply of oil cannot be retained, such as open bearings or gears.

Grease is a fine dispersion of an oil-insoluble thickening agent - usually soap in a fluid lubricant which is generally mineral lubricating oil. The soap is made up of fatty acid, tallow or vegetable oil saponified with alkali which can be hydrated lime, caustic soda, lithium hydroxide or aluminum hydroxide. The lubricating oil component is refined base oil-naphthenic, of medium viscosity index, or cylinder oil stock. Structurally grease is a water-in-oil emulsion. Its appearance is smooth, mostly translucent, soft or hard.

Properties essential for performance of grease are structural stability, lubricating quality, low and high temperature performance (which are provided by the selected lube oil base stock), where as properties such as water resistance, high temperature quality, resistance to break down through continuous use and ability of grease to stay in place are provided by the soap.

Additives e.g. Graphite, modified clay, asphalt, oxidation and corrosion inhibitors, extreme pressure additives molybdenum disulphide etc. are used to impart specific properties as required by end application.

Factors to be considered when selecting greases are the type of grease, which in turn depends on operating temperatures, water resistance, oxidation stability etc. The second factor, no less important, are the grease's characteristics, including viscosity and consistency.

The value of plastic lubricants has been recognized since very early times when animal fats were used for Axles and the like.

In general any lubricating fluid can be gelled by means of a suitable thickness to form a lubricating Grease. In practice mineral oils are almost exclusively used. For soap type Greases mineral oils of relatively low viscosity index 60 are preferred since the greater solvency of the more aromatic oils for soaps makes manufacture easier and gives greases with lower soap contents and with better properties.

Synthetic Fluids: Esters and silicones are used, only in greases for special applications, where cost is secondary to performance to meet low temperature and high temperature requirements; - 75C to + 320C.

The Soaps used are the metallic salts of long chain fatty acids derived from wide range of natural fatty materials. Soaps are mainly produced by specifying the fat or fatty acid with appropriate alkali in the presence of oil.

In some cases pre-formed soaps are used, such as aluminium stearate, lithium sterate etc.

Non Soap Thickners may be inorganic e.g. silica or clay or organic with a very high melting point . e.g. terephthalamates, arylureas (these may be either pre-formed or formed in situ) and the dye stuffs, indanthrene and phthalscyanine. They need to be oleophilic and this characteristic may be imparted either in the thickner formulation (i.e. by including a long chain hydrocarbon chain or surface esterification ) or by coating the particle surfaces with organic cations. In the latter case about 75 percent of the particle surface is covered, which gives the desired effect without affecting inter particle forces too much. Pre-treated clays (i.e. coated and dried) need aids to facilitate dispersion in oil. These dispersion aids are low molecular weight polar organic compounds such as methanol, acetone, diacetone Alcohol and propylene Carbonate.

A satisfactory Grease for a given application is expected to:

  1. Provide adequate lubrication to reduce friction and to prevent harmful wear of bearing components
  2. Protect against corrosion
  3. Act as a seal to prevent entry of dirt and water.
  4. Resist leakage dripping or undesirable throw off from the lubricated surfaces.
  5. Resit objectionable change in structure or consistency with mechanical working (in the bearing) during prolonged services.
  6. Not stiffen excessively to cause undue resistance to motion in cold weather.
  7. Have suitable physical characteristics for the method of application.
  8. Be compatible with elastomer seals and other materials of construction in the lubricated portion of the mechanism.
  9. Tolerate some deqree of contamination, such as moisture, without loss of significant characteristics.

Soap Greases consist of dispersions of soap fibres in oil in concentrations mostly in the range 5 to 22%. By weight sometimes solid block greases contain 50 to 40% of soap.

The thickeners in non-soap greases are usually particulate rather than fibrous in nature and in this case the structure is maintained by 3 dimensional linkages due to very short range inter particle forces (Vander waals forces). These linkages are readily broken and re-formed.

Types Of Greases

The metallic radical of the soap largely determines the characteristics of the greases the fatty radical having a secondary effect. Greases are therefore classified in terms of the metal they contain.

Calcium Soap Greases Sodium Soap Greases

The conventional types ( excluding the complex soap greases have a smooth buttery texture and are water resistant, with dropping points around 90- 100 C. They are water stabilized, that is , the water is present in the soap crystals as water of crystallization. The optimum amount of water varies considerably with the type of formulation, fatty material and mineral oil used, but is usually within the range of 0.5 1.3% by wt. at high temperatures the water is gradually lost and the soap structure is weakened. Consequently, calcium soap Greases are restricted to use at fairly low maximum temperatures about 50 60C. They all turn fluid after exposure to high temperatures and may separate into the oil and soap phases. Only those which contain other stabilizers besides water ( e.g. wool grease) will regain their structure on cooling.

These are usually more or less fibrous in structure/ texture depending mainly on the nature of the fatty material, high unsaturation yielding very fibrous greases. They have high dropping points usually not less than 150C and sometimes as high as 200C and are useful for relatively high temperature service. Owing to the solubility of the soap in water they are not water resistant.

 
Lithium Soap Greases Aluminium Soap Greases

These greases first appeared during -the World War II and were made from Lithium Stearate preformed soap. Now a-days lithium hydroxy stearate greases made by saponification in situ from hydrogenated castor oil predominate. Depending on the composition Lithium greases are smooth or slightly grainy in appearance. They have the highest dropping point about 190C of the conventional greases and the highest service temperatures. They are water resistant, mechanically stable, and can be made with a greater variety of types of oil than other greases. Their versatility and wide operational scope especially in high-speed service has led to their use as Multipurpose greases to the displacement of earlier types of more specialized greases.

Aluminium Greases have an attractive translucent smooth and polished appearance. The dropping points are low about 90C and the greases tend to become rubbery at high temperatures. They are almost invariably made from high viscosity oils and often incorporate polymers. Such products are water Resistant; stringy, and adhesive, and find application as chassis and gear lubricants. They are not recommended for rolling bearings.

 
Mixed Soap Greases Complex Soap Graeses

A variety of mixture is used, the commonest being Sodium-Calcium and the greases are generally manufactured by saponifying the fatty materials with mixed alkalies derived from different metals. One of the soaps usually predominates and determines the general character of the grease, while the other modifies the structure in some way. This results for example, in changes in texture and improved mechanical stability.

The normal soaps can be complexed with various inorganic salts, usually short-chain aliphatic compounds. The commonest type is a calcium soap calcium acetate complex although many other combinations have been patented. The greases are water resistant and have very high dropping points, in the range 200 -300C. With EP additives incorporated they are encountered as steel mill greases. New greases have recently been introduced for multi-purpose.

 
Non- Soap Greases

There are two main types, these intended for general industrial use and those for specialized applications. The former include greases thickened with silica and clay ( Bentonite) and organic derivatives,such as terephthalamates, diamido dicarbonyl and aryl substituted ureas. High temperatures, mechanical stability, water resistant etc. suggest that they are multipurpose greases with a wider scope than soap greases. However, they have not made any great impact on the market. The type used for specialized applications includes greases made from the dye stuffs indanthrene and phthalocyanine which are generally combined with synthetic fluids, such as diesters and silicones and hence are very expensive. One such product is claimed to operate between - 75C and + 320C.

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Solvent Based Resin Plants

What is Resin ?

Resins are film forming materials used in the production of paints and coatings. It binds the pigment particles into a coherent film that adheres to the substrate. The quality of the resin used in the production of paints and coating decides the durability of the paint. Resins are used depending upon the functional properties of the paint.

Functions of Resin:

To provide gloss and elasticity.

For the suspension of pigments.

To provide resistance to water, chemicals and abrasion.

Makes coating adhere to the surface.
Acts as a dispersant.
For drying properties.

Alkyd resins from the largest group of synthetic resins are used in paint industry. Most air drying enamels are based on long or medium oil alkyd resins. These resins dry at room temperature and have excellent flow and leveling properties, good exterior durability and can be thinned with mineral turpentine. Oils used for producing alkyd resins are linseed oil, soybean oil and Dehydrated Castor Oil (DCO).

Plant Operations:

Frigmaires solvent based plant produces paints, coatings, stains, and surface treating products at a rate of about 1.1 million gal/yr. This paint manufacturing plants operations primarily involve blending and mixing of raw materials, product testing and packaging and cleaning of vessels and lines. Color separation of the product is done to befit customer specifications.

Water-based and solvent-based paints are mixed in different tanks from 200- to 1000-gal capacity. The material used in water-based paints include water, latex, resins, extenders, and dispersed pigments. For solvent-based paints, the materials are generally similar in type, but solvent replaces water and latex. Other ingredients used in this base include plasticizers, tints, and thinners.

After batches are made up, they are transferred to the let-down tanks. Additional water (or solvent), resins, preservatives, anti-foaming agents, thinners, and bactericides are added thereafter in the tanks. Batch testing encompasses checking color, viscosity and gloss. The material are then filtered and charged to cans for labeling, packaging, and shipping.

Waste Generation:

The principal waste streams are the result of equipment cleaning, especially from water-based paints. For example, rinsing the let-down tanks ordinarily requires about 35 gal of rinse water, but that amount increases to 53 gal if light paint is to be blended after dark paint. The hazardous nature of water rinses results from the mercury used as a bactericide in the paint.

The rinses are separated from the paints according to the color intensity. Waste rinses that are not reused are piped to holding and flocculation tanks, after that alum is added to lower the pH and flocculent is added to precipitate some solids. Finally, the supernatant liquid is removed for reuse in other paint formulations.

The tanks are rinsed with mineral spirits at a rate of about 5 gal/400-gal tank. There after, the washings are sent off-site for recovery, followed by recycling or sale as fuel.

Waste Minimization;

In addition to reusing rinse water and recovering solvent, following measures to reduce waste generation are specified below :

Cleaning of the equipment before paint dries and hardens.
Eliminating hazardous materials.
Avoiding hazardous container waste by collecting the bactericide in water-soluble bags.
Scheduling batch formulations so that light colored paints precede dark ones.

Reducing the inventory of raw materials to avoid degradation and spoilage and to ensure a high-quality product.

Using bag filters for collecting dust.

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Acralic Resin Plants

What are Emulsions:

Emulsions are solvent free binders used in the preparation of paints and coatings. These are produced by the polymerization process where monomers are dispersed in an aqueous phase to get a uniform and stable emulsion. Paints and coatings based on emulsion systems are best in performance and are environment friendly.

Functions of Emulsion:

Excellent binding and hardness properties.
Makes the paint elastic.
Better sheen and gloss.
Excellent U.V. resistance.

High pigment loading capacity.

Acrylic Emulsion in Paints:

Different types of emulsions used in paints are pure and styrene acrylic emulsions. These emulsions are economical and are easily available. Emulsion based paints are free of solvents and are fast replacing solvent based paints due to its functionality and environmental friendly properties.

Manufacturing Process:

The processes involved in the formation of acrylic emulsion resin are complex and vary extensively. The production of low molecular weight dispersant product generates significant quantities of wastes.

Acrylic Emulsion Production:

Different acrylic emulsion formulations are produced by frigmaires acrylic emulsion resin plant. The steps involved in acrylic emulsion production varies greatly from product to product. Steps involved in the production of acrylic emulsion are listed below:

Raw materials for the emulsion line include monomers, additives, activators, and catalysts in liquid or solid form. For stabilization, some monomers are pre-mixed with inhibitors.

Catalysts are used for activating the monomers and initiating the desired reactions. Activators activate the catalysts, initiates the reaction, besides overcoming the effects of the inhibitors. Additives used in the mixture include detergents, dispersants, and pH-adjustment ingredients.

There after, the monomers are pumped from tanker trucks to monomer tanks for storage.

From the storage tanks, monomers are pumped to holding / premixing tanks, additive, activator, and catalyst holding tanks where mixing occurs.

The additives, activators, and catalysts can be directly added to the reactors without being mixed with monomers in their respective holding tanks.

Then, the raw materials are mixed together in one of three temperature- and pressure-regulated reactors where polymers are formed. The desired chemical reactions are initiated by addition of catalysts and are regulated with additives or by pressure and temperature adjustment.

The resulting acrylic emulsion polymers are pumped to blend tanks. Formalin is added in the blend as a preservative to control bacteria and mold growth and ammonia is added to for pH adjustment. Sodium hydroxide is another pH-adjustment chemical, added in the blend tanks.

Ingredients such as emulsions, emulsifiers, surfactants, binders and thickeners are added to modify monomer viscosity, to stabilize the polymers and to hold the polymers in suspension.

Finally, deionized water is added to lower the solids content. After each polymer batch is processed, the blend tanks are flushed with deionized water which is further pumped to the plant's wastewater treatment system.

Wastes generated during different processes include composited absorbed monomers, burnable liquids, and off grade methylolacrylamide / acrylamide. Most of the composited absorbed monomer waste are generated from spillage during loading and unloading of the rail cars or from batch spills and reactor clean-ups.

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Multipurpose Resin Plants

Pilot Plant:

Multipurpose Resin Plants are the pilot plants of Frigmairies. The structural design, configuration and material of construction of our plants can be custom made to suit the distinct requirements of our clients. These plants can produce both solvent and acrylic based resins.

Capacities of our Multipurpose Resin Plant range from 10 to 100 Ltrs. / Batch. Frigmairies can provide operation and installation support at the client's location, if required. Our design and technical engineers assist you about the proper functionality of our plant.

The precision configuration of our Multipurpose Resin Plant are specified below:
Reactors:

The reactors that are configured in our plant are manufactured as per ASME codes. These reactors are developed from superior quality stainless steel ranging from 1000 Ltrs. The capacity of these reactors is Upto 2, 000 ltrs. Specially designed agitators with heating coils / jackets upto 350C are configured in our reactors. Internal colding can also be taken care.

Heat Exchangers:

Thermic fluid heating systems upto 3 Million KCAL / Hr with all ancillary equipment and safety requirements are offered by us. Further, we also provide steam generators, having capacity of 1000 Kgs / Hr.

Condenser:

We provide you with distinct choices in the condenser types, to befit our customer's requirements. These can be configured in the plant to befit your specific requirement. The material of construction of these condensers can also vary in accordance to distinct need.

We offer following choices in our condensers :
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Shell & Tube, U Bundle Type
Fixed or Floating Head Type
Double Pipe Coolers
M.O.C: Stainless Steel, Carbon Steel, Monel, Nickel Aluminum
Filtering:

Specially designed filtering units for micron size filtering are incorporated on our plants. The resins and emulsions that are produced in Frigmairies Multipurpose Resin Plant comply with the industrial standards. The waste material generated during the production process is efficiently filtered and separated with the help of these filtration units.

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Sigma Kneader

Excellent for kneading and mixing of highly viscous materials like dough, putty, rubber solutions, adhesives, polymers etc. The mixing action is a combination of smearing, stretching, folding, dividing and recombining as the material is processed between the sigma blades and the container walls. Jacket arrangement is provided for heating or cooling application. In bigger models the container is tilted by a hydraulic cylinder to ensure complete discharge of mass.

MODEL TOTAL VOLUMETRIC CAP. IN LTRS. HP HYDRAULIC TILTING HP
SK 6 6 1.5 N.A
SK 25 25 3 N.A
SK 50 60 5 N.A
SK 125 125 10 N.A
SK 225 225 20 1.5
SK 500 500 30 2
SK 1000 1000 60 3
SK 1500 1500 75 3
SK 3000 3000 300 7.5
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